Graphite E Beam Crucibles

Overview of High-Purity Graphite Crucibles for E-Beam Evaporation

High-purity graphite crucibles are an integral component of e-beam evaporation systems, offering superior performance and longevity. MetalsTek provides graphite crucibles designed to enhance deposition efficiency and ensure consistent results across multiple evaporation cycles.

Benefits of High-Purity Graphite Crucibles

  • Thermal Efficiency:
    Graphite crucibles act as an effective thermal barrier between the melt and the water-cooled hearth.

    • Enhanced Deposition Rates: Deposition rates can increase by up to 400% at the same power level compared to a bare hearth.
    • Reduced Power Requirements: For the same deposition rate, power consumption can be reduced to 25% of the bare hearth’s power.
  • Purity Standards:
    Each crucible undergoes rigorous purification to meet exacting purity levels:

    • Major contaminants like Fe, Si, Al, and Mg are reduced to less than 5 ppm.
    • No detectable levels of 16 other common metals, including Na, K, and Pb, ensuring clean evaporation.
  • Durability:
    Graphite crucibles are built to withstand as many as 400 evaporation cycles, making them a cost-effective choice for high-volume operations.

  • Material Compatibility:
    These crucibles are compatible with a wide range of materials, including:

    • Metals: Cr, Cu, In, Mg, Mo, Pt, Ta, Ti, Zn
    • Alloys: Al-Ge, Al-Si
    • Compounds: CdS, Na₃AlF₆, SiO₂, Y₂O₃
  • Customization Options:

    • Taller crucibles hold more material but are unsuitable for multi-hearth furnaces not designed for their dimensions.
    • Model EVCEB-2 includes a top lip and has the same dimensions as EVCEB-4.

Important Note: These ultra-fine-grain, high-density graphite crucibles are distinct from “glassy” or vitreous carbon, which often cracks after just one use.

Common Causes of Crucible Breakage

To maximize the lifespan of your graphite crucible, it is crucial to avoid these common issues:
1. Incorrect Ramp/Soak Settings
E-beam evaporation recipes rely on carefully managed ramp/soak power levels to gradually heat materials to the desired deposition temperature:
  • Power Control Transition: During deposition, control shifts from ramp/soak settings to a PID loop. This loop manages the e-gun power supply and quartz crystal controller to maintain the deposition rate.
    • Oscillating Power Levels: If ramp2/soak2 levels are far from the required deposition power (e.g., 1 Ångström/sec), the PID loop compensates erratically, causing power fluctuations between +90% and 0%. These wild swings rapidly liquefy and condense the material, stressing the crucible and leading to cracks.
    • Solution: Ensure ramp2/soak2 levels are close to the deposition power level, reducing PID adjustments and preventing rapid phase changes.
2. Abrupt Power Shutdowns
Handling the power supply improperly after deposition can also damage the crucible:
  • Rapid Cooling Stress: Turning off the power abruptly or using a short ramp-down period causes the melt to solidify quickly. This rapid solidification induces mechanical stress on the crucible, potentially causing breakage.
    • Preventive Measure: Implement a gradual ramp-down process to allow for even cooling, reducing stress on the crucible liner.

Graphite E Beam Crucibles

Item No. Angle Drawing Capacities (mL) Top Diameter A (mm/inch) Height B (mm/inch) Wall Thickness C (mm/inch) Inquiry
EVCEB-1 angle=30 View Drawing
1 19.1 (0.75") 4.1 (0.16") 1.0 (0.04")
EVCEB-1A angle=15 View Drawing
1 14.2 (0.56") 9.8 (0.38") 2.4 (0.09")
EVCEB-2 angle=15 View Drawing
2 17.9 (0.71") 11.8 (0.47") 2.4 (0.09")
EVCEB-3 angle=15 View Drawing
3 20.4 (0.81") 13.8 (0.55") 2.4 (0.09")
EVCEB-4 angle=15 View Drawing
4 22.0 (0.87") 14.3 (0.56") 2.4 (0.09")
EVCEB-4A angle=15 View Drawing
4 22.5 (0.89") 15.1 (0.60") 2.4 (0.09")
EVCEB-7 angle=15 View Drawing
7 29.6 (1.17") 14.3 (0.56") 2.4 (0.09")
EVCEB-7A angle=15 View Drawing
7 28.6 (1.13") 13.2 (0.52") 2.4 (0.09")
EVCEB-10 angle=15 View Drawing
10 35.2 (1.38") 15.1 (0.59") 2.4 (0.09")
EVCEB-12 angle=15 View Drawing
12 32.5 (1.28") 23.9 (0.94") 2.4 (0.09")
EVCEB-12A angle=15 View Drawing
12 34.3 (1.35") 17.. (0.68") 3.2 (0.13")
EVCEB-12B angle=15 View Drawing
12 33.9 (1.33") 19.5 (0.77") 2.4 (0.09")
EVCEB-15 angle=15 View Drawing
15 37.6 (1.48") 17.0 (0.67") 3.2 (0.13")
EVCEB-15A angle=15 View Drawing
15 37.6 (1.48") 17.0 (0.67") 6.4 (0.25")
EVCEB-16 angle=15 View Drawing
16 41.7 (1.64") 24.6 (0.97") 3.2 (0.13")
EVCEB-20 angle=15 View Drawing
20 42.5 (1.67") 19.5 (0.77") 2.4 (0.09")
EVCEB-25 angle=15 View Drawing
25 47.0 (1.85") 17.3 (0.68") 2.4 (0.09")
EVCEB-25A angle=15 View Drawing
25 41.5 (1.63") 23.9 (0.94") 2.4 (0.09")
EVCEB-25B angle=15 View Drawing
25 47.0 (1.85") 17.3 (0.68") 3.2 (0.13")
EVCEB-25C angle=15 View Drawing
25 41.5 (1.63") 23.9 (0.94") 3.2 (0.13")
EVCEB-30 angle=15 View Drawing
30 45.1 (1.78") 23.9 (0.94") 2.4 (0.09")
EVCEB-30A angle=15 View Drawing
30 45.1 (1.78") 23.9 (0.94") 6.4 (0.25")
EVCEB-30B angle=15 View Drawing
30 48.8 (1.92") 20.6 (0.81") 2.4 (0.09")
EVCEB-35 angle=15 View Drawing
35 52.9 (2.08") 19.5 (0.77") 2.4 (0.09")
EVCEB-40 angle=15 View Drawing
40 51.6 (2.03") 25.9 (1.02") 2.4 (0.09")
EVCEB-40A angle=15 View Drawing
40 51.6 (2.03") 25.9 (1.02") 6.4 (0.25")
EVCEB-40B angle=15 View Drawing
40 50.8 (2") 27.0 (1.06") 2.4 (0.09")
EVCEB-40C angle=15 View Drawing
40 50.8 (2") 27.0 (1.06") 6.4 (0.25")
EVCEB-62 angle=15 View Drawing
62 56.2 (2.2") 35.6 (1.4") 2.4 (0.09")
EVCEB-62 angle=15 View Drawing
100 68.6 (2.7") 37.8 (1.49") 2.4 (0.09")
EVCEB-156 angle=15 View Drawing
156 82.6 (3.25") 38.9 (1.53") 6.4 (0.25")
EVCEB-A angle=15 View Drawing
N/A 23.8 (0.93") 15.1 (0.59") 2.4 (0.09")
EVCEB-B angle=15 View Drawing
N/A 75.2 (2.96") 39.7 (1.56") 2.4 (0.09")
EVCEB-C angle=15 View Drawing
N/A 60.7 (2.39") 25.4 (1") 6.4 (0.25")
EVCEB-D angle=15 View Drawing
N/A 48.0 (1.89") 17.8 (0.7") 3.2 (0.13")

Graphite E Beam Crucibles

EVCEB-40B

EVCEB-40C

Graphite E-Beam Crucibles

EVCEB-156

Graphite E-Beam Crucibles

Graphite E-Beam Crucibles

EVCEB-12A

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